Language : English
Xiangdong Hu

Paper Publications

Divergent Synthesis of 17-nor-Cephalotane Diterpenoids through Developed Ynol-diene Cyclization

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Impact Factor16.1

DOI number:10.1002/anie.202407757

Journal:Angew. Chem. Int. Ed.

Abstract:17-nor-Cephalotane diterpenoids include two categories, Cephalotaxus troponoids and tropone-free 17-nor-cephalotane diterpenoids, which possess polycyclic frameworks with seven-membered A ring bearing different oxidation states. We report herein a novel ynoldiene cyclization as a rapid access to tropone unit. Combining with a bioinspired stereoselective dual hydrogenation, the first divergent strategy to both categories of 17-nor-cephalotane diterpenoids has been successfully established, which enabled the total synthesis of Cephalotaxus troponoids, (+)-3-deoxyfortalpinoid F and (+)-harringtonolide, and tropone-free 17-nor-cephalotane diterpenoids, (−)-fortalpinoids M/N/P and analog (−)-20-deoxocephinoid P, in 14-17 linear longest steps starting from commercially available materials.

Indexed by:Journal paper

Page Number:e202407757

Translation or Not:no

Included Journals:SCI

Links to published journals:https://onlinelibrary.wiley.com/doi/full/10.1002/anie.202407757

Correspondence Author:Xiangdong Hu